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Prevalence of malnutrition was 34%. Materials and methods: This is a descriptive retrospective study, aiming to characterize the prescribing policy for human albumin in the population over 64 years of age, admitted in the Internal Medicine ward, within January 1st and December 31st, 2016. Princeton, NJ May 2007 Melvin A.
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Abstract Studies of the surface assembly and molecular organization of organic thin films were studied using scanning probe microscopy SPM and scanning probe lithography SPL. Systems of organic thin films such as n-alkanethiols and pyridyl functionalized porphyrins were characterized at the molecular level, and measurements of the conductive properties of polythiophenes containing in-chain cobaltabisdicarbollides were accomplished. Investigations of the surface assembly of 5,10-diphenyl-15,20-di-pyridin-4-yl-porphyrin DPP on Au 111 were done using SPL methods of nanoshaving and nanografting. Automated computer designs were developed for nanofabrication to provide local characterizations of the thickness of DPP films and nanostructures. Nanolithography was accomplished using DPP films as either matrix self-assembled monolayers SAMs or as molecules for nanofabrication. Results presented in this dissertation demonstrate that DPP forms compact layers on Au 111 , which can be used for inscribing nanopatterns of n-alkanethiols. Arrays of DPP nanopatterns with precise geometries and alignment were fabricated within n-alkanethiols by nanografting, demonstrating nanoscale lithography with pyridyl porphyrins can be accomplished to produce an upright surface orientation on Au 111 mediated by nitrogen-gold chemisorption. Beyond research investigations, the applicability of atomic force microscopy AFM and advancements with automated SPL were applied for teaching undergraduate chemistry laboratories to introduce the fundamentals of surface chemistry and molecular manipulation. Undergraduates were trained to prepare nanopatterns of n-alkanethiols using software to control the position, force and speed of the AFM tip for nanolithography experiments. The sensitivity and nanoscale resolution of current sensing AFM was applied for studies of the conductive properties of electropolymerized thin films of polythiophenes with cobaltabisdicarbollide moieties. Images acquired with AFM furnished views of the morphology of different polymers prepared on gold surfaces. Surface maps of the conductivity of electropolymerized films were acquired with AFM current images. These studies provide new insight of the effects of the bound cobaltabisdicarbollide moiety and coordinated metal centers for the electronic properties of the resulting conducting materials. At the end of the one year period, either we or LSU may request an automatic extension for one additional year. At the end of the one year secure period or its extension, if such is requested , the work will be released for access worldwide.
